I. A Study of Free Radicals. II. A Method for Determining the Structure of Organic Stannonic Acids and a New Method of Preparation of Organo-mercuri Compounds ... |
Common terms and phrases
acetone acid is added acid to litmus AgNO3 alcohol is removed Calc carbinol chloride in 50 chloroform crystalline Dilute hydrochloric acid dissociation electronegative ethane ethyl iodide ethyl stannonic acid fitted for steam flask for three flask is filtered free of stannous free radicals gentle evaporation glacial acetic acid Gomberg grams of stannous Grignard reagent hexa-arylethanes hydrochloric acid ion by repeated liter round bottom mercuric acetate mercuric chloride metachlorophenyl magnesium bromide METHOD OF PREPARATION methyl carbon atom methyl mercuric iodide methylene mixture is acid mixture is treated mole of metachlorophenyl ORGANIC STANNONIC ACIDS ORGANO-MERCURI COMPOUNDS peroxide phenyl radical potassium iodide preparation of ethyl PREPARATION OF ORGANO-MERCURI removed by gentle repeated centrifuging residual mixture round bottom flask sodium chloride sodium hydroxide sodium stannite stannonic acid separates stannous chloride stannous ion steam bath steam distillation stoppered flask sulfuric acid triphenylmethyl washed with water water are added water until free whole is shaken Yield