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aAlFeSi adherence of porcelain Aluminum Council ammonium chloride Angstroms Anodized antimony trichloride spall argon basic white lead-silicate Building Science Series Bureau of Standards chemical chromium Clean Chem cycle deoxidizer electron microprobe Elements enamel and fired enamel to aluminum enamel-metal systems enameled specimens enamels fired Fail Fail Fail Fail Fail Pass Fail Pass Pass fracture furnace atmosphere Gugeler indicated Laboratory Lead-Free magnesium silicide mechanisms of adherence Mg2Si mill addition National Bureau nitrogen oxide layer Pass Fail Fail Pass Fail Pass Pass Pass Fail Pass Pass Pass percent Pickle Pickle Pickle Pickled Prefired Pickled Porcelain Enamel Institute porcelain enameled aluminum potassium Prefire Pickle Pickle Prefire Pickle Prefire Prefire Prefire Pickle Prefire Prefire Prefire reaction products Round-robin testing scanning electron microscope spall failures spall resistance spall solutions Spall Test Results spall test solution studies systems that spalled Transmission Electron Microscopy trichloride spall test white lead-silicate enamel X-ray diffraction X-ray Powder Diffraction