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absorbance acetic acid alcohol aldehydes alkenes alkyl amine anhydride anhydrous aqueous aromatic beaker benzene benzyl boiling chip boiling point bromide carbon carbonyl chloride chromatography column components concentrated sulfuric acid cool to room crystals derivatives determine diethyl Dissolve distilling flask dropping funnel Erlenmeyer flask ester ethanol ethyl Experimental procedure filter flask fitted fraction give Grignard reagents groups halogen Heat the mixture hydrocarbons hydrochloric acid hydrogen identify infrared iodide ketones laboratory layer liquid melting point mixture under reflux mole n-butyl NaOH solution nitrate nitrobenzene obtained oil bath optically active organic compounds oxidized phenols precipitate preparation pressure protons react reactivity Recrystallize reduced reflux condenser residue room temperature round-bottomed flask sample separatory funnel simple distilling head SN2 reactions soft flame solid solubility solvent spectra spectroscopy spectrum stirring substances suction filtration sulfuric acid tertiary test tube vapor wash yield and melting