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3-cyclohexenyl carbinol acetic acid acetolysis acid liberated alcohol LXI aliquots Anal anchimeric assistance anhydrous anhydrous acetone anhydrous ether anhydrous magnesium sulfate aqueous acetone borneol camphene carbinyl tosylate carbon atom Chem complex was broken corresponding saturated crystallised cyclohexyl Cyclohexyl carbinol dihydro a-terpineol dilute hydrochloric acid Dimethyl distillation gave double bond dried over anhydrous ester ether solution ether was added evaporated formation formic acid formolysis heat of combustion hexenyl hydrochloric acid hydrogen hydrolysis ice-cold dilute hydrochloric iso-propyl chloride Kcal kgat l-methyl-3-cyclohexenyl layer limonene lithium aluminum hydride LXXII magnesium iodide magnesium sulfate methanol method methyl magnesium iodide moles neighboring group participation order rate constants palladium on charcoal para-nitrobenzoates para-toluenesulfonic phenyl lithium prepared product analysis rates of solvolysis ratio reaction mixture refluxed reported residue on distillation saturated alcohols secondary alcohols sodium hydroxide solvent steam bath stirred terpinolene tertiary alcohols Tertiary Chlorides tion tosylate Tosylate Tosylate trans unreacted ester unsaturated values