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acetate acetonitrile acetylene acetylene derivs added dropwise alcohols aldehydes aldimines aliphatic alkyne allyl amines Angew anhydride argon aryl asym benzyl bromide carbonate carboxylic acid esters catalyst Chem chiral complexes cyclic cycloaddition dichloromethane Diels-Alder reaction enantioselectivity Engl enolate epoxidation Et3N ethers ethylene ethylene derivs extra C-atoms F.e. incl fluoride glycosides groups halides hydride hydrogen ibid induction intermediate intramolecular iodide ketones ligand Lithium methyl methylene chloride Michael addition microwave irradiation mild conditions mixture of startg mixture stirred N-acylation N-protected nitriles nucleophilic oxidation oxo compds Palladous Perkin Trans phenols phosphine polymer-based synthesis Potassium prim procedure pyridine quenched with satd radical reactant 60 reagent 60 reduction refluxed regio regiospecific ring closure room temp salts silyl Sodium solvent startg stereospecific stirred at room Synlett Synth Synthesis 2000 synthesis 60 Tetrahedron 56 Tetrahedron Lett Tetrahedron:Asym THF added toluene triflate trifluoroacetic