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20 grams acetaldehyde acid chlorides Action of titanium added slowly addition compound addition product alcohol on titanium aluminium chloride ANALYSIS Found Calculated anhydride of acetic attempt to prepare benzene calcium chloride carbon tetrachloride chloride was evolved compounds formed contain oxygen cooled titanium tetrachloride decomposed by water decomposition Demarcay described dichloro-titanic acid dissolved distillate consists double compound dried and analyzed ether on titanium evolution of hydrogen excess titanium tetrachloride flask formula fractionally distilled Friedel glacial acetic acid grams of titanium heating hydrogen chloride hydrolyzes in moist iso-amyl alcohol lead tetra-ethyl Levy8 mercury ethyl methyl alcohol mixed anhydride mixture moist air n-butyl alcohol nineteen hundred Ohio State University organic compounds partially decomposed phenyl bromide precipitate reaction product red oil reflux condenser silicon tetrachloride solid which melts soluble in alcohol substance tetrachloride was poured TiCls TiClsOR TiCU titanium tetra titanium trichloride water bath white solid writer has prepared yellow crystalline solid yellow solid