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acetate acid solution 50 add 10 ml alloy steels ammonia ammonia solution approximately beaker boiling calibration caustic soda caustic soda solution chromium Clarke's solution Cool cupferron degreased determined dilute to exactly distillation evaporate filtrate free tin g of potassium g of sample g of sodium graduated flask hot water hydrochloric acid s.g. hydrochloric acid solution hydrogen ignite iodide mercury minutes ml of hydrochloric ml of nitric ml of sulphuric ml of water ml with water molybdenum niobium nitric acid s.g. oxide oxidised oxygen perchloric acid potassium bromate potassium iodate potassium iodate solution potassium permanganate potassium permanganate solution precipitate Principle The sample residue silica silver nitrate sodium arsenite sodium carbonate sodium thiosulphate Special reagents specimen standard potassium iodate standard sodium sulphuric acid sulphuric acid s.g. sulphuric acid solution temperature tin coating weight tinplate titrate Total coating weight Transfer tungsten vanadium volume ml wash solution water and dilute wt g