Models for the synthesis of linear metallic oligomers: The bis(diorganohalotin) tetracarbonylosmium system. The [[3,3'-(trimethylenedinitrilo)-di-2-butanone dioximato] (1-)] rhodium system, Parts 1-2
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14H total added addition products adduct alkyl halides Amer Anal anion benzene blue solution boron bridged bubbled butanone Calcd carbon tetrachloride carbonyl Chem cobalt colorless compounds crystals cyclohexyl di-2-butanone dianion dichloride 25 dichloromethane dihydride 3_ dioximato dioximato](l-)]rhodium electron ethanol excitonic filtered and washed formed Found give the product hexane hydrogen chloride Inorg KBr pellet ligand mechanism mercuric chloride metal metal bonds methyl mixture was stirred mmol molecule nitrogen nmr 60 MHz nucleophile organotin osmium oxidative addition oxidative addition reactions oxime bridge phenyl planar 27_ polymer polymerization precipitate proton Raman reaction mixture reactivity recrystallized recrystallized from dichloromethane rhodium room temperature short silica gel silica gel silica gel column sodium borohydride solid solvent stereochemistry superconductivity THF 5 ml tin complexes tin hydrides trans-bis triphenylphosphine triphenyltin chloride unsaturated 27 vacuum warmed to room washed with ether yield