Report on the Results of the ICES/IOC/OSPARCOM Intercomparison Exercise on the Analysis of Chlorobiphenyl Congeners in Marine Media--step 1, and the Intercomparison Study of the Determination of CBs in Baltic Herring Oil
International Council for the Exploratio of the Sea, 1992 - Biphenyl compounds - 78 pages
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80 laboratory ampoules Annex Aroclor B(day based on peak BASELINE blank broken horizontal line capillary columns carrier gas CB concentrations CB congeners chlorinated chlorobiphenyl congeners chromatograms were returned coefficient of variation coeluting concentrations with 95 CP-Sil csi csi csi rA D(day detector determination dilutions dimethylpolysiloxane Duinker electron capture detector eluting fish oil gas chromatography GC conditions GC/MS guidelines horizontal line shows ICES ICES/IOC/JMG intercalibration identified intercomparison exercise internal standard iso-octane isomerids IUPAC laboratories were able laboratory number Figure linear range linearity curves marine media Mean concentrations Netherlands optimization optimum Organochlorine outliers participants peak areas peak heights polychlorinated biphenyls prediction-interval twice rA csi results based results for CB ro ro sample SE-54 column shows the true splitter closing standard deviation standard solutions statistical evaluation Table twice the standard versus the laboratory YE5 YE5 YE5