Preparation and Reduction of M-nitrostyrylquinoline and Some Stilbazoles and Related Compounds ... |
Contents
DESCRIPTION OF RESULTS | 6 |
mNitroXstilbazole | 22 |
Catalytic Reduction of mNitroxstilbazole Methiodide | 36 |
2 other sections not shown
Common terms and phrases
acetic anhydride alcohol to give aldehyde analysis was conducted antimalarial approximately Attempted Catalytic Reduction bazole benzaldehyde brown crystals carbinol CH₂ CH3 CH3 Chem color condensing agent conducted by Huffman cooling gave crystals melting crystals were formed dark red distilled dried due to leakage ethyl alcohol filtering and drying filtrate fractionating column g of m-nitrobenzaldehyde hot alcohol hydriodic acid hydrochloric acid hydroxide ibid ice bath m-nitro malaria melting point methyl iodide mg CO₂ mg sample gave milk of magnesia mixed melting point mixture was filtered mixture was refluxed ml of alcohol orange parasites picoline piperidine platinic oxide platinum potassium pounds of hydrogen product obtained pyridine quinaldine methiodide quinine quinoline Raney nickel catalyst reaction mixture reaction product recrystallization from alcohol refluxed round bottom flask sealed tube sintered slightly soluble styrylquinoline substance temperature theoretical tin and hydrochloric viscous water-cooled condenser white crystals white needles Y-Picoline Methiodide Y-picoline XI yield zinc chloride zole