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acetic acid concentration Acid Disproportionation acidity function acyloin alcohol Anal aqueous authentic sample base degradation benzene bismuthate Calcd carbonyl carbonyl peak catalyst Chem compound XXIV crude product degradation product dialdehyde XXVIII diamide XXXI Diels-Alder Adduct Dihydro-3,5-dicarbethoxy-2,6-lutidine XXIV dihydrocompound dihydropyridine dimethylpseudopelletierine methiodide XXI diol XXXII dissolved distilled dried over magnesium end product ester ethanol ethanolic hydrochloric acid evaporation extracted flask fractions Graph hydrochloric acid hydrogen chloride hydroxide Infrared maxima infrared spectrum ketone kinetic lithium aluminum hydride lutidine LVIII magnesium sulfate mechanism Meinwald melting point methyl mole nitrogen obtained optical density original ketone overnight oxidative p-Benzoquinone p-nitroaniline petroleum ether postulated precipitate prepared product showed protons pseudopelletierine methiodide Raney nickel rate constant reaction mixture recrystallization reduced pressure refluxing room temperature Semi-micro Hydrogenation semicarbazone sodium bismuthate Sodium Borohydride solution was dried solvent spectra starting material Tetracyanoethylene Thiobenzophenone tion tropinone ultraviolet absorption XXVI yellow yield