Solid State NMR Studies of Biopolymers

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Anne E. McDermott, Tatyana Polenova
John Wiley & Sons, Oct 11, 2010 - Science - 592 pages
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  • The field of solid state NMR of biological samples [ssNMR] has blossomed in the past 5-10 years, and a cohesive overview of the technology is needed for new practitioners in industry and academia
  • Provides an overview of Solid State NMR methods for studying structure dynamics and ligand-binding in biopolymers
  • Offers an overview of RF pulse sequences for various applications, including not only a systematic catalog but also a discussion of theoretical tools for analysis of pulse sequences
  • Includes practical examples of biochemical applications, and detailed discussion of the many aspects of sample preparation and handling that make spectroscopy on solid proteins successful
  • This book is an EMR Handbook – a spin-off from the Encyclopedia of Magnetic Resonance containing new and existing articles from the Encyclopedia
  

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Contents

Rue de la Doua Villeurbanne 69100 France
5
John S Waugh
29
Stefan Becker Department of NMRbased Structural Biology Max Planck Institute
39
Grant
49
E Raymond Andrew
83
Douglas P Burum
99
Tatyana Polenova Department of Chemistry and Biochemistry University of Delaware
111
Recent Developments in SolidState NMR Hardware and Emerging
139
Relaxation Studies of Solid Biopolymers
343
Spectral Analyses
359
Numerical Simulations in SolidState NMR with SIMPSON
377
Protein Structure Calculation Using Ambiguous Restraints
395
Protein Structure Calculation and Automated NOE Restraints
405
Christopher P Jaroniec Department of Chemistry Ohio State University Columbus OH 43210
413
Structural Studies
417
Structural Studies by MAS
433

William W Brey National High Magnetic Field Laboratory Florida State University
141
HighFrequency Dynamic Nuclear Polarization
159
Homonuclear Dipolar Recoupling in SolidState
175
Heteronuclear
189
Adiabatic PolarizationTransfer Methods in MAS Spectroscopy
213
SymmetryBased Pulse Sequences in MagicAngle Spinning SolidState
229
DipolarBased Torsion Angle Measurements for Protein Structure Determination
273
Structure and Dynamics Studies by MAS SolidState
285
Correlation Spectroscopy for Resonance Assignments in SolidState Proteins Using Jcouplings
297
Indirect Coupling and Connectivity
317
Fast MagicAngle Spinning for Protein SolidState NMR Spectroscopy
331
Structural Studies of Protein Fibrils and Misfolded Proteins by SolidState
447
Structural and Dynamics Studies of Lipids by SolidState
463
An Overview
473
SolidState NMR Studies
491
Photosynthetic Antennae and Reaction Centers
509
Structure and Function Studies of Energy and Signal Transducing Proteins by SolidState
517
Therese Malliavin Unite de Bioinformatique Structurale Institut Pasteur 2528 Rue
519
ProteinSolvent Interactions in Solids
525
Unifying Solution and SolidState NMR Studies of Nucleic Acid Dynamics
535
Index
553
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About the author (2010)

Anne McDermott is Senior Lecturer in English at the University of Birmingham.

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