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2-bromobutanoate acetic acid acetyl added aecondary amine alcoholic solution ALIPHATIC alkyl halide aminea ammonia anilide aniline aides aqueous Aster bath beiling bensyl chloride benzene benzyl besore carbon carbonyl catalyst Chea Chem chlcride CO2CH3 I I cryetale dimethylamine dissiculty distillation disubstituted ester dried dropping sunnel dry ether eith eptical etber ethereal solution flask equipped Grignard reagent groupa heure houra hydrogen hydrolysis ice-ccld lamine liquid boiling mcle melting methanol methyl iodide mixture wae mole N-methyl-n-butylamine nitrogen obtained one-hals optical peint potassium carbonate potassium hydroxide potassium permanganate primary aminé product pthalimide reaction mixture reduction resluxed sor saponisi secondary siltrate slask sodium hydride sodium hydroxide solution sollowing sor neutral sor sive sor sorty-eight sor the Degree sormation sormed sree radicale stand sor sulsate tbe original ester tbe preparation tertiary amine thia triphenylmethylsodium srom trisubstituted acet washed with water whicb yielded