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2.4 litres per 93.5 litres per acetate acetylene flow Acid Cycle apparatus approx azeotrope BIOS boiled carbon dioxide carbon-carbon carbonyl group catalyst solution charged circulating reaction system cold complete oxidation composition concentration of nitric condensate cooling corrosion dangerous to handle developed diagram dissolved distillation Dr.Schimmelschmidt emulsion ester explosion extract feed or nitric feed tank flow of acetylene freezing point German heating hydrogen peroxide hydroxide and hydrogen impurities Kilos per day laboratory last traces liquid nitrogen dioxide litres capacity litres per hour McKee mercuric nitrate mercury method methyl acrylate methyl ketone metres high mixed acid mixture nit reform nitration vessel nitric acid Nitrofona optimum organic compounds Pauling column potassium hydroxide prepared nitroform pure purification column purification tower purity quantity react reaction liquid reaction product reaction vessel recovery reduced pressure reflux regenerated run-off SCALE Schimmelschmidt believed scrubbed scrubber separation and concentration sodium Square sulphuric acid synthesis temperature tetranitromethane with potassium tne reaction trinitro unsaturated warm