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acetic acetone acetonitrile Acrolein aldehydes amino acids Anal.Chem band broadening benzaldehyde capillary capillary column car exhaust carbonyl carbonyl compounds cell volume Chemical concentration conventional HPLC Crotonaldehyde dansyl hydrazine dansylated sugars derivatives derivatization derivatization procedure detection limit detector cell dichloromethane dimedone DNPH reagent Dns-Cl DNS-hydrazones EKLUND eluent emission excess reagent excitation extraction falling jet Figure flow rate fluorescence detection fluorescent responses formaldehyde fructose GC/GC/EC gradient elution hexane HPLC HPLC systems hydrazine hydrolysis increase injected isocratic Johnson JOSEFSSON laser laser beam laser-induced fluorescence liquid chromatography MARSTORP AND G methanol method mL/min mmol mobile phase mol/L Mopper NBD ethers NBD-Cl NBD-Hyp NBD-OCH NBD-OCH2CH2OH Nucleosil optimal organic solvent phase mode postcolumn precolumn derivatization propanal quantitative quartz quartz capillary reaction conditions reaction mixture reacts reagent reagent solution reversed phase HPLC sample volume scattered light selectivity sensitivity separation Seppak solubility Table technique trace analysis tube wavelengths yields