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200 cc flask 500 cc three Adam's catalyst alpha picoline methiodide amide had formed ammonia had evaporated ammonium hydroxide ammonium iodide amount of ferric atom benzene benzyl chloride bromine butanol-1 cc of concentrated cc of liquid cc of water cc three necked CH CH CH chloroform chromium trioxide compound cooled crystals that melted dilute dissolved distilled dried dropping funnel ethanol ether extracted ferric nitrate g and melted g of ammonium g of sodium heated hour hydrochloric acid isoquinoline l-amino-3-methylisoquinoline liquid ammonia mechanical stirrer melted from 64 methiodide was added methyl group methyl iodide methyl iodide 60.0 methylene base mg sample gave mixed melting point mixture necked flask fitted oxidation placed a solution potassium amide pseudo base pyridine methiodide quaternary salts quinaldine methiodide quinoline reaction recrystallized small amount sodium amide sodium hydroxide sodium nitrite solution became stirrer was placed sulfuric acid three necked flask water was added x-nitro-3-methylisoquinoline yield