Advanced ESR Methods in Polymer Research
Wiley, Sep 18, 2006 - Science - 353 pages
A definitive work on ESR and polymer science by today's leading authorities
The past twenty years have seen extraordinary advances in electron spin resonance (ESR) techniques, particularly as they apply to polymeric materials. With contributions from over a dozen of the world's top polymer scientists, Advanced ESR Methods in Polymer Research is the first book to bring together all the current trends in this exciting field into one comprehensive reference.
Part I establishes the fundamentals of ESR, from experimental techniques to data analysis, and serves as a valuable overview for the beginning ESR student. Part II introduces the broad range of ESR applications to polymeric systems, including living radical polymerization, block copoly-mers, polymer solutions, ion-containing polymers, polymer lattices, membranes in fuel cells, degradation, polymer coatings, dendrimers, and conductive polymers. By exposing readers to the great potential of ESR, the authors hope to encourage more extensive application of these methods.
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ContinuousWave and Pulsed ESR Methods
Double Resonance ESR Methods
Calculating SlowMotion ESR Spectra of SpinLabeled
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acid acrylic alkyl analysis angle anisotropic axis basis set calculated chain length Chem coatings components conductive polymers copolymer correlation corresponding counterions cross-linked CW ESR D-band degradation dendrimers detected dimeric distance distribution doped dynamics echo effect electron spin Electron spin resonance ENDOR ESEEM ESR spectra ESRI experimental exposure frequency fuel cell function g-tensor Gerlock gradient groups HALS HPEC hyperfine coupling hyperfine splittings increase ionomers ions irradiation isotropic Jeschke line width Macromolecules Magnetic Field measured melamine membrane model radicals molecular molecules MOMD motion Nafion nitroxide nitroxide concentration nitroxide radicals nuclear spin nuclei observed obtained oxidation oxygen paramagnetic parameters photoinitiation rate Phys polaron polyelectrolyte polymer chain profiles propagating radicals protons pulse radical polymerization relaxation resonance rotational diffusion sample Schlick shown in Fig signal simulated solution solvent spectroscopy spectrum spin label spin probes spin trapping stability structure surface surfactant tensor thermal tion transition values Zeeman