Advances in Magnetic Resonance: The Waugh Symposium

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Warren S. Warren
Academic Press, Dec 2, 2012 - Science - 308 pages
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Advances in Magnetic Resonance: The Waugh Symposium, Volume 14 is a collection of manuscripts presented at the 1989 symposium on “High Resolution NMR in Solids , held at the Massachusetts Institute of Technology. The contributors provide 20- to 30-page articles consistent with AMR’s traditional emphasis on quantitative analysis of NMR techniques.
Organized into 13 chapters, this book discusses the principles triple-quantum filtered two-dimensional exchange spectroscopy and its application in the measurement of cross correlation between pairs of dipole-dipole interactions. It then describes alternative ways of using fictitious spin in pulsed nuclear quadrupole resonance or NMR. General topics on the application of optical spectroscopy; the saturation of spin-spin energy by slow continuous bulk rotation; the frequency-switched Lee-Goldburg pulse cycle; and high-resolution proton NMR in solid systems are also explored. A chapter examines an entirely different view of spin dynamics in the presence of radio-frequency fields. This book also deals with the theoretical background and application of solid-state and zero-field NMR spectroscopies to structure determination. Lastly, the utilization of the Floquet formalism in the design of broadband propagators in two-level systems and the two classes of novel NMR phenomena related to the symmetrization postulate are discussed.
Analytical and quantum chemists, physicists, biochemists, and materials science researchers will find this book invaluable.
 

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Contents

Chapter 1 Measurement of Dipole Dipole Cross Correlation by TripleQuantum Filtered TwoDimensional Exchange Spectroscopy
1
Chapter 2 Assessment and Optimization of Pulse Sequences for Homonuclear Isotropic Mixing
35
Chapter 3 Spin12 Description of Spins 32
59
Chapter 4 Optical Pumping Measurements of Nuclear Cross Relaxation and Electric Doublets
75
Chapter 5 Spin Relaxation and Saturation in Solids by Quasiadiabatic Transformations
95
Chapter 6 FrequencySwitched LeeGoldburg Sequences in Solids
111
Chapter 7 HighResolution H Nuclear Magnetic Resonance in Solids via CRAMPS
125
A DressedStates Viewpoint
151
Chapter 9 Structure Determination by SolidState Nuclear Magnetic Resonance Spectroscopy
183
Chapter 10 ZeroField Nuclear Magnetic Resonance Entirely in High Field
203
Chapter 11 Floquet Formalism and Broadband Excitation
219
Chapter 12 Applications of Shaped Pulses to HighResolution Nuclear Magnetic Resonance in Dipolar Broadened Spin Systems
241
Chapter 13 The Symmetrization Postulate and Nuclear Magnetic Resonance of Reacting Systems
269
INDEX
293
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Warren is affiliated with Princeton University, New Jersey.

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