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F Infrared Spectroscopy
H Radiochemical Methods
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Abstr acetic acid acetyl acetyl chloride added alcohol aldehydes aliquot amines Anal analysis Analytical Chemistry Analytical Data anhydride apparatus azeotropic distillation back-titration benzene boron trifluoride buret calculated catalyst cell CH3OH Chapter Chem chloride co-workers compounds concentration coulometric cyclohexanone dead-stop Determination of Water determining water dimethylformamide dioxane direct titration distillation dried dry methanol electrodes electrometric equivalent esterification esters excess extraction free water given in Table glycol hydrate hydrogen hydrolysis hydroxyl iodine Karl Fischer reagent ketones KFR method KFR titration liquid mercaptan methanol methyl mg of water mixture ml of dry mole oven drying oxide percent water peroxide platinum pretitrated procedure pyridine quantities react reaction Reprinted with permission resin room temperature salt samples containing shown in Table sodium solution solvent standard water-in-methanol stopper sulfur dioxide technique tion titer titrated with KFR titration flask tube visual endpoint volumetric flask water content Water found weight