Chiral Separations: Methods and Protocols
Gerald Gübitz, Martin G. Schmid
Springer Science & Business Media, 2004 - Science - 448 pages
Prominent experts from around the world detail the chromatographic and electroseparation techniques they have developed for chiral separations on an analytical scale. Described in step-by-step detail to ensure successful experimental results, the procedures are presented as either general methods or as specific applications to substance classes and special compounds, with emphasis on high performance liquid chromatography and capillary electrophoresis techniques, but also including thin layer chromotographic, gas chromatographic, supercritical fluid chromatographic as well as recent electrochromotographic techniques.
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acetate acetonitrile amine amino acids amylose Anal analyte application aqueous Armstrong aromatic capillary electrochromatography capillary electrophoresis carboxylic acid cellulose Chem chiral recognition chiral resolution chiral selector chiral separation chiral stationary phase Chiralcel Chiralpak Chirobiotic Chro Chromatogr chromatographic separation coating column complexes concentration crown ether CSPs cyclodextrin cyclodextrin CSPs derivatives derivatization detector diastereomers Dissolve drugs electrolyte eluent elution enantiomer separation enantioselectivity filling technique filter flow rate groups Gübitz HPLC hydrogen bonding hydrophobic imprinted injection interactions isomers ligand macrocyclic macrocyclic antibiotic matogr methanol Methods and Protocols migration mixture mobile phase Molecular molecules monolith monomers nonaqueous normal phase mode Note optical organic modifier packing peptides polar organic mode polymer polymerization polysaccharides prepared protein racemic reaction reagents retention reversed-phase mode ristocetin Schmid selectivity separation of enantiomers silica gel sodium solvent teicoplanin temperature thin-layer chromatography tion vancomycin