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Discussion of Results
Synthesis of 67Dihydro45benzhydrin
8 other sections not shown
acetic acid acetic anhydride acetyl chloride acid chloride acid hydrolysis Acidification ammonium benzoate Anal aqueous Bachmann benzene Braun and Reutter Calcd carbon catalyst cent Chem coloration with ferric compound Condensation of Tetralone condensation product COOCH cooled crude half-ester crystallized cyclization dehydrogenated dibasic acid dissolved distilled double bond ester ether gave ether left ether solution extracted with ether ferric chloride Fieser and Gates Found give grams Haberland hydrobromic acid hydrochloric acid hydrolysis hydrolyzed ibid isomers itaconic acids ketone ketone VII ketone XIX lactone Linstead Llichael melting point methanol Michael product mole naphthylpropionic acid neutral oil neutral portion obtained oxidation petroleum ether phenanthrene potassium hydroxide potassium hydroxide solution propionic acid pyridine pyrotartaric acid recrystallized refluxed residue taken ring Robinson and Schlittler room temperature semicarbazone sodium bicarbonate sodium bicarbonate solution sodium ethoxide sodium hydroxide soluble succinic ester sucoinonitrile sulfuric acid synthesis tert-butyl alcohol tetralone yield zinc chloride