Defense Technical Information Center, 1973 - 87 pages
The report covers work on the study of possible high temperature superconductors. It describes theoretical work on filamentary organo-metallic materials - the conduction mechanism, band theory, and screening; progress towards the synthesis of metallic chain compounds and related organo-metallic complexes, and experimental studies of their solid state properties. (Author).
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Abarbanel air sensitive alkyl halides Amer Anal band benzene bromide Calcd calculated carbonyl CDC1 chain Chem CO)cRe-Ge-Ge-Cl complex compounds Cyanine cyclohexyl dichloride dimethoxyethane DOH system electrons ethanol ether excess excitonic filtered Found gap equation gap function gave Ge-Ge bond germanium hexane hydrides indicated inert atmosphere box Infrared intermetallic intermetallic polymers iodide isolated ligand linear material MeCOS MeOAc metal atom metal cluster metal-metal bond methyl MHz in CDCl ml of THF mmol mmole molecular molecules Naval Research nmr 60 MHz obtained oxidative addition oxime oxime bridged parameters Phys Plane preparative TLC proton reacted reaction recrystallized reflux Rh(C?DOBF_ rhenium rhodium rhodium DOH sample Semi-Annual Technical Report silica gel singlet solid solution solvents spectra structure substrate sulfur Superconductors synthesis synthetic temperature THF was treated thioacetate trans transition metal unit cell W. A. Little X-ray yellow crystals yield