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Generation and Detection Techniques
The Reactions of Singlet Oxygen
4 other sections not shown
20 torr acetone alcohol allylic allylic hydroperoxides Amer aqueous sodium carbonate Chem chloride concerted ene mechanism configuration crude determined deuterated deuterium diastereomeric dichloromethane dilute aqueous sodium dioxetanes distillation double bond dried MgSO dropwise electronic ether was added ethyl ethylene phenyl phosphite ethylene phosphorochloridite evaporation expected flask formation gas chromatography hydrochloric acid hydrogen hydroperoxides ibid ice-cooled involvement isomer kinetic lifetime of singlet mechanistic mesylate methanol ml of dichloromethane ml of ether ml of water mmole mole molecular oxygen MTPA esters nitrogen nmr CCl nmr spectra o_-phenylene observed obtained olefin optical rotation oxidation oxygen evolution pathway pentane perepoxide intermediate perprotiated phosphite ozonides phosphorus trichloride Photooxygenation procedure employed pseudorotation pyridine rate constants rates of decomposition reaction mixture reaction of singlet resonances room temperature rubrene saturated aqueous sodium singlet oxygen sodium carbonate solution solvent stirring structure substituent substrates tion trimethylene triphenyl phosphite triphenyl phosphite ozonide yield