Sourcebook of Advanced Organic Laboratory Preparations

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Academic Press, Dec 2, 2012 - Science - 352 pages
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In the case of students, this laboratory preparations manual can be used to find additional experiments to illustrate concepts in synthesis and to augment existing laboratory texts. A name reaction index is also included to direct the reader to the location where specific reactions appear in this manual.
The industrial chemist is frequently required to prepare a variety of compounds, and this manual can serve as a convenient guide to choose a synthetic route.

Key Features
* Offers detailed directions for the synthesis of various functional groups
* Includes up-to-date references to the journal literature and patents (foreign and domestic)
* Reviews the chemistry for each functional group with suggestions where additional research is needed
* Name reactions are indexed along with the preparations cited
 

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Contents

Introduction
1
PARAFFINIC AND AROMATIC
4
CHAPTER 2 OLEFINS
16
CHAPTER 3 ACETYLENES
24
CHAPTER 4 ALCOHOLS AND PHENOLS
28
CHAPTER 5 ETHERS AND OXIDES
34
CHAPTER 6 HALIDES
41
CHAPTER 7 ALDEHYDES
49
CHAPTER 25 ENAMINES
208
CHAPTER 26 YNAMINES
211
CHAPTER 27 UREAS AND POLYUREAS
213
CHAPTER 28 CARBODIIMIDES
218
CHAPTER 29 NCARBAMATES URETHANES
221
CHAPTER 30 OCARBAMATES
228
CHAPTER 31 IMINES
234
CHAPTER 32 AZIDES
237

CHAPTER 8 KETONES
53
CHAPTER 9 CARBOXYLIC ACIDS
58
CHAPTER 10 ESTERS
83
CHAPTER 11 AMIDES
92
CHAPTER 12 CYANATES ISOCYANATES THIOCYANATES AND ISOTHIOCYANATES
106
CHAPTER 13 AMINES
117
CHAPTER 14 HYDRAZINE DERIVATIVES HYDRAZONES AND HYDRAZIDES
136
CHAPTER 15 DIAZO AND DIAZONIUM COMPOUNDS
147
CHAPTER 16 NITRO COMPOUNDS
156
CHAPTER 17 NITRILES CYANIDES
166
CHAPTER 18 MERCAPTANS SULFIDES AND DISULFIDES
175
CHAPTER 19 SULFOXIDES
182
CHAPTER 20 SULFONES
186
CHAPTER 21 SULFONIC ACIDS
189
CHAPTER 22 ALLENES
194
CHAPTER 23 ORTHO ESTERS
197
CHAPTER 24 SULFITES
202
CHAPTER 33 AZO COMPOUNDS AND AZOXY COMPOUNDS
243
CHAPTER 34 ACETALS AND KETALS
250
CHAPTER 35 ANHYDRIDES
258
CHAPTER 36 MONOALKYL SULFATES
267
CHAPTER 37 AMIDINES
273
CHAPTER 38 IMIDES
275
CHAPTER 39 OXIMES
278
CHAPTER 40 HYDROXAMIC ACIDS
284
CHAPTER 41 POLYMER PREPARATIONS
288
Documentation of Product and Process Research and Development
303
Document 1 Record Keeping Fact Sheet American Chemical Society
306
Document 2 Instructions for Keeping Laboratory Records Rohm and Haas Company
308
Document 3 CRD Laboratory Notebooks Du Pont de Nemours Company
318
Document 4 Electronic Record Keeping for Patent Purposes American Chemical Society
321
Name Reaction Index
325
Subject Index
327
Copyright

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About the author (2012)

Dr. Stanley R. Sandler won the R&D 100 Award offered by the industry in 1990 for a significant commercial process to prepare an important organic intermediate. In addition to this honor, he has over 100 publications involving patents, books, an encyclopedia article, several journal articles, and he is currently a referee for several journals. Sandler received his Ph.D. in Organic Chemistry from Penn State University.

Wolf Karo was a winner of the Westinghouse Science Talent Search. He holds a number of patents, and has been active in developing applications of monodispersed microspheres in diagnostic testing and other areas of biotechnology. Karo received his Ph.D. in Organic Chemistry from Cornell University.

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