Spot Tests in Organic Analysis
Development, present state and prospects of organic spot test analysis; Spot test techniques; Preliminary tests; Detection of characteristic functional groups in organic compounds; Identification of individual organic compounds; Application of spot reactions in the testing of materials, examination of purity, characterization of pharmaceutical products.
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FOREWORD vn CHAPTER 1 DEVELOPMENT PRESENT STATE AND PROSPECTS OF ORGANIC SPOT TEST ANALYSIS
SPOT TEST TECHNIQUES by PH W WEST
Laboratory and equipment requirements
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acetaldehyde acetic acid acid solution Acta added alcohol aldehyde aliphatic alkaline solution ammonia ammonium Anal aniline aromatic amines benzene benzidine blue color carbon disulfide carboxylic acids Chem chloride color appears color reaction concentrated sulfuric acid condensation containing cyanide detected dilute dissolved drop dyes esters ethyl evaporation Feigl filter paper filter paper moistened fluorescence formaldehyde formation formed groups guanidine heated hydrazine hydrochloric acid hydrogen hydroxide ketone Limit of identification micro crucible micro test tube Mikrochim minutes mixture nitrate nitric nitrogen nitrous acid orange organic compounds oxalic acid oxamide oxidation oxine peroxide phenols positive response potassium precipitate present Procedure react reagent paper reagent solution residue salicylic sample sensitive small amounts sodium solid soluble solution is treated solvent spot plate spot test analysis sulfate sulfide sulfonic sulfuric acid taken to dryness temperature test solution tube is covered unpublished studies urea violet color volatile warmed yellow yield