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Preparation of Dooosene1
Conversion of Olefines into Corresponding
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acetate alcohol aliyl alkali alkyl allowed to stand Amide Bale BBhme Böhme boiling British French bromide butanol butyrone Chem Chim chlorosulfonic acid compounds concentrated sulfuric acid condensed dehydrohalogenation detergent Deutsche Hydrierwerke dihexyl dilute dissolved distilled in vacuo distilled water ester ethylenes fatty acids fifty grams filtered flask following fractions fractionated in vacuo fractions were obtained gave Geigy German grams halides halogen heated Henkel hundred grams hydrolysis hygroscopic I. G. Subclass layer was evaporated lyophilic group methanol methyl molecular weight nickel carbonate Oil was treated olefines oxide palmitate Percent bromine percent whiteness potassium hydroxide previously prepared propanol-1 quaternary ammonium salts Rabtex reaction refluxed residue Silver Dust soap sodium carbonate sodium hydroxide sodium salt sodium sulfate solution stand overnight Subclass Subclass H sulfonates sulfuric acid Swiss tension theory thionyl chloride toluene triethanol amine unsaturation v/ith wash tests washed with water water layer water was added yield