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alkali metals alkaline earth iodides alkyl amounts of iodine analysis for barium anhydrous aqueous solutions BaIa barium iodide benzene Briggs and Patterson C.W. Mason calcium iodide cesium Chalker combined iodine composition coordination number coworkers crystals at concentrations CsI3 CsI4 decomposed determined by extrapolation distillation method outlined distilling flask evidence exist in sol expect the polyiodide experimental free iodine Grace halides halogen Herz hexagonal higher poly higher polyiodides hydrate hydrolysis hygroscopic indicated iodide and iodine Iodide Dihydrate iodide solution iodine atom Jakowkin least a week Metal Polyiodides Methods of Analysis monoclinic obtained by Rivett oxidizing agent Percentage Iodine phase diagram polyhalide Polyiodide Formation polyiodide of ammonium polyiodide of hydrogen potassium iodide range of concentrations ratio recrystallized reported Rivett and Packer rubidium salt sample Sidgwick sodium thiosulfate solid in equilibrium solid phase solid polyiodides solubility curve solvent T.G. Rockow theor titration unstable acids ution water solution ysis