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acetic adsorbent alcohol alkenes alkyl allowed anhydrous apparatus aqueous aromatic atoms bath benzene boiling point bond bottle Buchner funnel calcium chloride capillary carbon carbonyl catalyst cent Chem chemical shift chromatography column commercially components compounds concentrated condenser containing cooling desiccator dichloromethane dissolved distillation dried dropping funnel ethanol ether evaporate Expt extraction filtration flask fraction frequency fume cupboard ground glass joints heating hydride hydrogen hydroxide inserted ketones laboratory liquid magnetic melting point method methyl ml of water molecular molecule nitrogen Organic Chemistry oxide peaks peroxide plate potassium prepared pressure procedure protons pump purified quantities reaction mixture reagent recrystallisation reflux region removed round-bottomed flask rubber sample Section shown in Fig sodium sodium borohydride sodium hydroxide solid soluble solution solvent spectra spectrum stirrer stirring stopcock stopper suitable sulphate sulphuric acid surface synthesis syringe technique temperature tetrahydrofuran tion toluene tube vacuum vapour vibration washed