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200 reflection absorption corrections adjustment agreement analysis apparatus axis bakelite Bragg angle Bragg spectrometer brass briquet c-axis collimator Cone conical crystal Cornell CORNELL UNIVERSITY counter counting rate crystal table curves determination diffracted intensities dimensional analysis equivalent oxygen planes equivalent reflections experimental filament Havighurst height hkl and khl hko reflections inasmuch insulator integrated intensities intensities reflected intensity differences ionization chamber Laue method micrometer mounted number of counts observed oil box orystal oscillation photograph oxygen atoms position powder materials powder measurements ratio reflection obtained regular bipyramidal results obtained rotation photograph scattering material scattering power screw slit system sodium atom Sodium chloride sodium periodate space group spectrometer measurements structure amplitudes structure factors tetragonal thyratron tion total number unit cell variation vernier scale voltage wsre x-ray beam x-ray tube