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absorption Acta Cryst alignment angle appear approximation asymmetric unit atoms axes bond lengths Bragg's law calculated camera center of symmetry centrosymmetric Chapter coefficients coordinates correct corresponding crystal rotation crystal structure derived determined diffractometer direct effect electron density equations errors Figure film Fourier Fourier series glide heavy atoms indices intensity International Tables large number lattice lines lattice point located M. J. Buerger matrix measured method mirror plane molecules monoclinic normal observed obtained orientation origin orthorhombic oscillation parallel Patterson function peaks perpendicular phase point group possible precession problem r.l. point radiation reciprocal lattice refinement rotation axis scale scattering factor screw screw axis shown in Fig shows space group sphere of reflection structure factors superposition symmetry elements synthesis Tables for X-ray techniques thermal parameters tion triclinic unit cell usually values vector Weissenberg photographs Wiley X-ray Crystallography zero zero-level