Understanding Single-Crystal X-Ray Crystallography

Front Cover
John Wiley & Sons, Mar 8, 2010 - Science - 831 pages
Endlich ein Lehrbuch der Röntgenkristallstrukturanalyse von Einkristallen, das ohne weitreichende Vorkenntnisse in Mathematik auskommt! Theorie und methodische Grundlagen werden logisch strukturiert und gut verständlich dargestellt; der Band ist in sich geschlossen und erfordert keine Zusatzliteratur.
Für Studenten oberer Semester, Diplomanden und Doktoranden sowie zum Einstieg für Anwender aus allen naturwissenschaftlichen Disziplinen.
 

Selected pages

Contents

Understanding SingleCrystal XRay Crystallography Dennis W Bennett
67
Theory
195
Experiment
265
Data
339
Experimental
497
Statistical
571
Crystal Structure Refinement
673
Appendix
747
Determination of the Phase Parameter in the Amplitude
753
EA Discussion of Kinematical Models for Extinction
763
G Monte Carlo Optimization A Simple Example
773
Taylor Series
787

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Understanding Single-Crystal X-Ray Crystallography
Dennis W. Bennett
No preview available - 2010

Common terms and phrases

absorption ac plane amplitude assigned asymmetric unit atom atom locations average Bravais lattice calculated Cartesian centrosymmetric components constrained coordinate system cos² create crystal structure Crystallography detector determine diad diad axes diad rotation diagonal diffracted beam diffraction condition direct lattice displacement displacement vector electric field electron density enantiomorph energy equation Fourier fractional coordinates function glide planes heavy atom illustrated in Fig incident beam indices integral intensity intersection inversion center lattice point magnitude matrix maxima mirror plane molecule monoclinic multiple observed origin oscillators parallel parameters Patterson function Patterson map peaks perpendicular photons point group positions radiation reciprocal lattice vector refinement reflection resulting rotation axis scattering factor screw axis sin² space group sphere starting set structural solution structure factor symbol symmetry elements symmetry operations symmetry-equivalent transformation triplet relationships unit cell variables variance wave X-ray xf yf zf zero

About the author (2010)

Professor Dennis W. Bennett is a Professor of Chemistry and a member of the Laboratory for the Surface Studies at University of Wisconsin in Milwaukee. His research focuses on the physical-inorganic chemistry of molecular devices and catalytic systems. He holds a BS in Biological Sciences and a PhD in Chemistry, both from the University of Utah, where he also did post-doctoral research in photocatalysis. In more recent years, he was a NIH Senior Fellow at the Medical College of Wisconsin, where he gained expertise in macromolecular crystallography. He has also served as Chair of the Department of Chemistry and Biochemistry at UWM, and as a program manager in Basic Energy Services at the U.S. Department of Energy. Prior to his academic career, he was a research chemist at Phillips Petroleum Corp., and has continued to serve as a consultant to a number of companies and government agencies throughout the U.S. He is the author of over 130 peer-reviewed research publications.

Bibliographic information

TitleUnderstanding Single-Crystal X-Ray Crystallography
AuthorDennis W. Bennett
Editionillustrated
PublisherJohn Wiley & Sons, 2010
ISBN3527326774, 9783527326778
Length831 pages
Subjects ›  › 

Science / Chemistry / General
Science / Chemistry / Inorganic
Science / Physics / Crystallography
Technology & Engineering / Materials Science / General
  
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