Microscale inorganic chemistry: a comprehensive laboratory experience
This text is intended to provide students with instruction and valuable laboratory experience in the often neglected area of inorganic chemistry. Divided into four main parts, the book covers chemistry of the main group elements, chemistry of the transition metals, organometallic chemistry, and bioinorganic chemistry. Recognizing the high cost of materials, difficulties in waste disposal, and dangers of toxicity, the authors have adopted a ``microscale'' approach to experiments in the book, thereby also reducing the time students spend in preparation. With over 45 experiments, Microscale Inorganic Chemistry incorporates the use of a broad sampling of elements and also covers such topics as laboratory safety, equipment, report writing, and literature searching.
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absorbed acid bond boron carbon carbonyl Chem CHEMICAL DATA Compound chemical shift chloride chromatography clay tile column complex Compound FW Amount condenser Craig tube crystals cyclopentadiene cylinder DATA Compound FW distillation electrons energy Erlenmeyer flask ethanol EXPERIMENTAL PROCEDURE ferrocene filter paper frequency FW Amount mmol glass harmful if swallowed heat Hirsch funnel hydrate inhaled Inorganic Chemistry Isolation of Product laboratory lecture bottle ligand liquid magnetic stirring bar magnetic stirring hot material melting point metal mg/kg microscale mixture mmol molecule nitrogen nuclei obtained orbitals organic Organometallic ORL-RAT LD50 oxidation Pasteur pipet phase prepared pressure reaction reference Required for Experiment round-bottom flask Safety Recommendations salt sample sand bath shown in Figure side arm signal skin sodium sodium amide sodium chloride solid solution solvent spectra spectroscopy spin stirring bar stirring hot plate stopcock suction filtration thermal toxic vacuum vapor Wiley Wilkinson's catalyst