The Thermal Properties of Transition-metal Ammine Complexes |
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Contents
INTRODUCTION | 1 |
EXPERIMENTAL THERMOANALYTICAL TECHNIQUES | 13 |
HEXAMMINECOBALTIII COMPLEXES | 37 |
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amine ammine complexes ammonia ammonium chloride ammonium fluoride anhydrous anion aquopentammine ATmin values cadmium(II Chem chloride complex chromium(III cobalt(II composition contained coordinated copper(II corresponded curve inflection deamination deamination reaction deaquation reaction decomposed decomposition diammine Differential thermal analysis dissociation products dissociation temperatures DTA curves effect to 225°C endothermic peaks ethylenediamine evolution of ammonia evolved exothermic formation formed furnace given in Fig H₂O halide higher temperatures Inorg investigated iodide kcal ligand Lobanov lose mass loss magnetic susceptibility manganese(II mass spectrometer mass-loss curves matrix metal mixture mole of complex mole of ethylenediamine mole of water molecules moles of ammonia Mori nickel(II nitrate nitrogen Nucl observed obtained oxide platinum(II pyridine pyrolysis residue rhodium(III shown in Fig similar spectrometer stoichiometry studied the thermal sulfate Temp temperature range TGA curves thermal analysis curves thermal dissociation reaction thermal stability thermoanalytical thiocyanate triammine type complexes vacuo W. W. WENDLANDT yield zinc(II