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Methods of XRay Analysis for Hexagonal Layered
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3m lines 3R phase a-axis alkali metal ammonia analysis anion anneal Appendix atomic scattering factor Bragg equation c-axis calculated chalcogen Chapter composition compounds conduction band cool crystallite Debye-Waller factor extinct four-layer function Guinier increases Intensity Fit intercalated samples intercalation complexes lattice parameters layered transition metal linewidth liquid ammonia low temperature lT phase measured metal atoms metal-rich mixed anion monoclinic NbSe NbSe2 NbSg niobium observed obtained octahedral octahedral coordination organic molecules phonon plane polytype powder preferred orientation Prism pyrex pyridine quenched reaction reciprocal lattice reflection registry shift samples prepared Section seen selenium selenium atoms single crystal slab thickness stacking disorder Stoichiometry structure factor sulfur superconducting transition temperature tantalum TaS_ TaS2 TaSe TaSe2 TaSg thermal transition metal dichalcogenides transport Trig tube UH(b Uh(c unintercalated material unit cell X-M-X slabs X-ray diffraction xSex