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Methods for the Determination of Water
Titrimetric Determination of Water Using Karl Fischer Reagent
Nature of the Karl Fischer Reagent
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acetic anhydride acetyl chloride acidimetric alcohol aldehydes aliquot amines Anal analysis analyzed anhydrous back titration boron trifluoride buret calculated carbonyl compounds cent water CH.COOH CH.OH Chapter Chem cyclohexanone determination of moisture Determination of Water dioxane direct titration distillation dry methanol electrodes endpoint equivalent esterification esters excess extraction Fischer reagent titration Fischer titration free water given in Table glacial acetic acid glass-stoppered volumetric flask glycol gram samples grams of boron hydrogen cyanide hydrolysis hydroxide hydroxyl Ibid iodine Karl Fischer reagent mercaptan methanol method methyl milliequivalents milligrams milligrams of water milliliter millimoles mixture moisture content mole of water nitriles obtained oven drying oxide peroxide present procedure pyridine quantities of water reacted reaction room temperature salt sodium solvent stoppered sulfur dioxide technique tion titer titrated directly titrated with Karl titration with Fischer trifluoride per liter tube volumetric flask water content Water found water-in-methanol