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1,3-pentadiene 15 mmol acetone acid addition adduct allyl anisole authentic samples benzene benzene-d butadiene butadiene and ethylene calcd carbon carbonyliron catalyst system Chem chloride CO2Me codimerization compounds coordinatively cyclization cyclopentadiene cyclopentadienyl)dicarbonyliron dimer cyclopentene degassed deuterium content dimer dimer 13 distilled double bond eluted endo ester ethanol ether ethylene evaporated exo hydrogen Fe(CO fluoborate formed gave heated at 100 hexadiene hexane hexane was photolyzed hydrogen hydrogen transfer intermediate iodide iodo ir-allyl iron complex isolated by preparative isomer isomerization isoprene l(exo ligand mass spectrometry Mass spectrum metal hydride methyl acrylate mmol nickel Nmr CC14 nmr tube olefin organometallic oxidation oxygen peak phosphine photolysis piperylene ppm error preparative glc column propylene proton ratio reaction resonance rhodium(III room temperature sealed under vacuum sequence showed absorptions solvent spectra styrene substituted side thermolysis tion tricarbonyliron triethylaluminum triphenylphosphine tube sealed tube was heated unsaturated vacuum line yield