Solid State NMR Studies of Biopolymers

Anne E. McDermott, Tatyana Polenova

John Wiley & Sons, Sep 20, 2010 - Science - 592 pages

The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI.

The field of solid state NMR of biological samples [ssNMR] has blossomed in the past 5-10 years, and a cohesive overview of the technology is needed for new practitioners in industry and academia. This title provides an overview of Solid State NMR methods for studying structure dynamics and ligand-binding in biopolymers, and offers an overview of RF pulse sequences for various applications, including not only a systematic catalog but also a discussion of theoretical tools for analysis of pulse sequences. Practical examples of biochemical applications are included, along with a detailed discussion of the many aspects of sample preparation and handling that make spectroscopy on solid proteins successful.

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The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks  are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

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Contents

• Rue de la Doua Villeurbanne 69100 France: 5
• John S Waugh: 29
• Stefan Becker Department of NMRbased Structural Biology Max Planck Institute: 39
• Grant: 49
• E Raymond Andrew: 83
• Douglas P Burum: 99
• Tatyana Polenova Department of Chemistry and Biochemistry University of Delaware: 111
• Recent Developments in SolidState NMR Hardware and Emerging: 139
• William W Brey National High Magnetic Field Laboratory Florida State University: 141
• HighFrequency Dynamic Nuclear Polarization: 159
• Homonuclear Dipolar Recoupling in SolidState: 175
• Heteronuclear: 189
• Adiabatic PolarizationTransfer Methods in MAS Spectroscopy: 213
• SymmetryBased Pulse Sequences in MagicAngle Spinning SolidState: 229
• DipolarBased Torsion Angle Measurements for Protein Structure Determination: 273
• Structure and Dynamics Studies by MAS SolidState: 285
• Correlation Spectroscopy for Resonance Assignments in SolidState Proteins Using Jcouplings: 297
• Indirect Coupling and Connectivity: 317
• Fast MagicAngle Spinning for Protein SolidState NMR Spectroscopy: 331
• Relaxation Studies of Solid Biopolymers: 343
• Spectral Analyses: 359
• Numerical Simulations in SolidState NMR with SIMPSON: 377
• Protein Structure Calculation Using Ambiguous Restraints: 395
• Protein Structure Calculation and Automated NOE Restraints: 405
• Christopher P Jaroniec Department of Chemistry Ohio State University Columbus OH 43210: 413
• Structural Studies: 417
• Structural Studies by MAS: 433
• Structural Studies of Protein Fibrils and Misfolded Proteins by SolidState: 447
• Structural and Dynamics Studies of Lipids by SolidState: 463
• An Overview: 473
• SolidState NMR Studies: 491
• Photosynthetic Antennae and Reaction Centers: 509
• Structure and Function Studies of Energy and Signal Transducing Proteins by SolidState: 517
• Therese Malliavin Unite de Bioinformatique Structurale Institut Pasteur 2528 Rue: 519
• ProteinSolvent Interactions in Solids: 525
• Unifying Solution and SolidState NMR Studies of Nucleic Acid Dynamics: 535
• Index: 553

About the author

Anne E. McDermott and Tatyana Polenova are the authors of Solid State NMR Studies of Biopolymers, published by Wiley.

Bibliographic information

• Title: Solid State NMR Studies of Biopolymers; Volume 2 of eMagRes Books
• Editors: Anne E. McDermott, Tatyana Polenova
• Edition: illustrated
• Publisher: John Wiley & Sons, 2010
• ISBN: 0470721227, 9780470721223
• Length: 592 pages
• Subjects: Science / Chemistry / General; Science / Spectroscopy & Spectrum Analysis