Synthetic Methods of Organometallic and Inorganic Chemistry
Wolfgang A. Herrmann
Georg Thieme Verlag, 1996 - Chemistry, Inorganic - 237 pages
The last in this ten-volume series, this text covers the most important standard compounds to be generally used in laboratories engaged in all branches of synthetic chemistry.
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1H NMR acid activity added addition allowed amount Anal analysis Angew Application aqueous argon aryl atmosphere autoclave calcd carbon catalyst cationic Chem colloid complexes compound concentrated containing conversion cooled crystals derivatives described dichloromethane diethyl ether dissolved distilled dried dropwise enantioselective ethylene evaporated extracted Figure filtered filtration formed Fraction functionalized Gas chromatographic give heated homogeneous hydrogen IH NMR increases Introduction isolated ligands material metal method minutes mixture is stirred mmol moisture nitrogen obtained organic Organomet oxidation pentane performed peroxide phase Polymerization powder precipitate precursor prepared pressure Procedure Properties pure reaction mixture reduced References removed residue resulting room temperature Scheme Schlenk selectivity silica slowly solid solution solvent sorbic stable starting stirred substrate supported suspension Synthesis Table toluene vacuum volume washed yellow Yield