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24 hours allotropic form analysis and X-ray analyzed as UF5 anhydrous hydrofluoric acid atomic ratio black crystalline clusters black cubic crystals black fluoride black material black UF4 called diuranium enneafluoride cent F chem chemical analysis Chicago preparation Chicago workers coarser color conditions of preparation decomposition pressure determined Distorted UF4 established by means Experiments exposing UF4 exposure extraneous lines forms of UF5 gave green UF4 Grosse's preparation hours pumping hydrate laboratory liquid UF6 Livingston MDDC number obtained Occurrence original black pentafluoride photogram pumping at 300°C sample showed Samples prepared Sin20 Int Table temperature tetravalent U content Theoretical composition titration total U2F9 and UF5 u4 F F/U UF4 Int UF4 prepared UF4 surface area UF5 UF6 UF6 pressure Union of Chemistry URANIUM FLUORIDE COMPOUNDS vapor pressure week weighing bottle weight gain weight loss white product X-Ray diffraction data X-ray diffraction pattern X-ray pattern X-ray studies Zachariasen