Mass Spectrometry: A TextbookThis book offers a balanced mixture of practice-oriented information and theoretical background as well as numerous references, clear illustrations, and useful data tables. Problems and solutions are accessible via a special website. This new edition has been completely revised and extended; it now includes three new chapters on tandem mass spectrometry, interfaces for sampling at atmospheric pressure, and inorganic mass spectrometry. |
Contents
1 Introduction | 1 |
2 Principles of Ionization and Ion Dissociation | 21 |
3 Isotopic Composition and Accurate Mass | 67 |
4 Instrumentation | 117 |
5 Practical Aspects of Electron Ionization | 222 |
6 Fragmentation of Organic Ions and Interpretation of EI Mass Spectra | 249 |
7 Chemical Ionization | 351 |
8 Field Ionization and Field Desorption | 381 |
10 Fast Atom Bombardment | 479 |
11 MatrixAssisted Laser DesorptionIonization | 507 |
12 Electrospray Ionization | 560 |
13 Ambient Mass Spectrometry | 621 |
14 Hyphenated Methods | 651 |
15 Inorganic Mass Spectrometry | 685 |
Appendix | 717 |
| 735 | |
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Common terms and phrases
accurate mass acid Adapted from Ref Anal Analysis analyte atmospheric pressure beam bond capillary carbenium ion cation Chap Chem Chemical Ionization Chemistry Chromatography cleavage cluster ions collision compounds Cyclotron detection detector dissociation effect electron ionization Electrospray Ionization emitter Example Fast Atom Bombardment Field Desorption fragment ions FT-ICR gas phase hydrogen interface ion formation Ion Proc ion source ionic Ionization Mass Spectrometry ionization methods isotopic patterns kinetic energy linear Liquid loss m/z value magnetic sector MALDI mass analyzer Mass Spec Mass Spectrom matrix Matrix-Assisted Laser Matrix-Assisted Laser Desorption/Ionization McLafferty McLafferty rearrangement metastable mode molecular ion molecules neutral NIST orbitrap peak at m/z peptide permission positive-ion precursor ion protein proton Quadrupole Ion Trap Rapid Commun reaction Reproduced from Ref resolution sample scan sector instruments signal solvent spectra spray surface Tandem Mass techniques thermal Time-of-Flight Time-of-Flight Mass tion trom trometry vacuum voltage